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Beilstein J. Org. Chem. 2020, 16, 2788–2794, doi:10.3762/bjoc.16.229
Graphical Abstract
Figure 1: a) The carbohydrate-based building block for the synthesis of stimuli-responsive surfactants. b) Th...
Scheme 1: Synthesis of 5 from levoglucosan (1).
Scheme 2: Functionalization of the building block 5β.
Scheme 3: Hydrolysis of the ethyl esters 12 and 13.
Scheme 4: Synthesis of compound 19 from building block 5.
Figure 2: 1H NMR titration of compound 19 with Zn2+ ions in acetonitrile-d3.
Figure 3: (1) 1:1 Mixture of 1-octanol/H2O, (2) same solvent mixture with compound 19, and (3) same solvent m...